产品描述
| Analysis Method | Product Specification | Product Result |
| Chemical Purity by HPLC/UV | ≥98% | 99.42% |
| Identity by 1H NMR | Conforms to Structure | Pass |
| Identity by 13C NMR | Conforms to Structure | Pass |
| Identity by Mass Spectrometry | Conforms to Structure | Pass |
| Isotope Incorporation by Mass Spectrometry | ≥98% D/Molecule | 99.68% |
| Intended Use |
| This material is intended only for laboratory use in analytical and R+D applications. It not suitable for human/animal consumption or for household use. |
| Hazards |
| Read Material Safety Data Sheet (MSDS) and understand any potential hazard(s) prior to the use of this product. All chemicals should be considered potentially hazardous in nature and should only be handled by qualified personnel using established good laboratory practices. |
Analytical Data
1. HPLC/UV
| Instrument: | Shimadzu LCMS-2020 |
| Column: | Eclipse XDB C18 4.6×250 mm, 5 μm |
| Mobile Phase: | A: 0.1% Formic acid in Water B: Acetonitrile |
| Gradient: | 88%B over 1 min, 88%～50%B from 1 min to 2 min, 50%～12%B from 2 min to 3.5 min, 12%～88% from 3.5 min to 4.5 min,maintain to 6 min |
| Flow Rate: | 1.0 mL/min |
| Wavelength: | 254nm |
| Acquisition Date: | December 6, 2018 |
| Peak # | Ret. Time (min.) | Area (mAU) | Height (mAU) | Area % |
| 1 | 2.602 | 17152 | 3592 | 0.576 |
| 2 | 2.755 | 2959140 | 627997 | 99.424 |
| Total |
| 2976292 | 631589 | 100.000 |
2. 1H NMR&13C NMR
| Instrument: | Bruker ANANCE 600MHz |
| Solvent: | CDCl3 |
| Acquisition Date: | December 6, 2018 |
