矿石应用-布鲁克微区X射线荧光

应用领域:地矿/钢铁/有色金属,地矿/钢铁/有色金属

检测样品:矿石

检测项目:矿石检测

参考标准:ASTMB568

方案摘要

State of the art micro-XRF applied to geological samples

Micro-XRF on geological samples M4 TornadoLarge samples (H×W×D:200mm×160mm×120mm)Powerful sample stage(100mm/s,5kg)Pre-Vacuum conditions for detection of elements down to NaPolycapillary optics for high excitation intensity and spot size<25 μmSDDs for detection/processing of over 100 kcpsVarious measurement modes(single-or multi-point,line scans,area scans)Optional 2nd X-ray tubeOptional 2nd detectorPosition Tagged Spectroscopy(HyperMap)Versatile"data-mining"softwareStandard-free quantification

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Scan of the Cetaceous/Paleogene boundary in Raton Basin US

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Thin sections measurements(64-bit OS)

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Trace elements in garent Thin section of a garent containing slateFull area map shows symmetric Mn core within the crystalsSelected garnet neasured extensively with strong primary filter to reduce background and to avoid Bragg diffraction peaks370 pixel×460 pixel→170000 pixel mapMeasurement time:1 s/pixelSteps:25μm

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SummaryUnique speed and perfoimance in the determination of the element distribution in large sample with measurement tiomes per pixel of 0.3 ms and up tp 4 Million pixels in a single Hyper MapHigh spatial resolution down to 25 μm X-ray spot size,motors steps of 4 μmOptimal for the analysis of inhomogeneous samples,due to better identification of the representative location of interestNon-destructive,fast analysis of large samples without preparation,including solid,power oe liquid samplesQualitative and quantitative analysis of all elements from Na upwards,due to vacuum chamber,detection limit for heavy trace elements in the low ppm rangeStandardless Fundamental Parameter quantification with type calibration optionPowerful Software with multiple tools for optimal data mining

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