71.040.40 化学分析 标准查询与下载

KS D 2055-2021 环氧模塑料中铅和镉的测定方法

Method for determination of lead and cadmium in epoxy molding compound

KS D 1791-2021 镍铁化学分析方法

Methods for chemical analysis of ferronickel

KS D 2054-2021 银浆中铅、镉的测定方法

Method for determination of lead and cadmium in silver paste

KS R 1301-2021 汽车用橡胶中铅、镉的测定方法

Method for determination of lead and cadmium in rubber for automobiles

KS D 2056-2021 汽车用铁氧体中铅、镉的测定方法

Method for determination of lead and cadmium in ferrite for automobiles

KS D 1942-2021 铜合金及铜制品中铬的测定方法

Methods for determination of chromium in copper alloys and copper products

KS R 1303-2021 车用火花塞中铅、镉的测定

Determination of lead and cadmium in spark plug for vehicles

NY/T 3870-2021 硒蛋白中硒代氨基酸的测定 液相色谱-原子荧光光谱法

Determination of selenoamino acids in selenoproteins by liquid chromatography-atomic fluorescence spectrometry

ASTM E3243-21 芬太尼和芬太尼相关化合物用现场检测设备和分析的标准规范

1.1?General:? 1.1.1?This specification provides system designers, manufacturers, integrators, procurement personnel, end-users, practitioners, and responsible authorities a common set of parameters to match the capabilities of chemical detection tools with user needs for their

Standard Specification for Field Detection Equipment and Assays Used for Fentanyl and Fentanyl-Related Compounds

ASTM E3290-21 确定芬太尼和芬太尼相关化合物现场检测设备和分析性能的标准试验方法

1.1?General:? 1.1.1?This test method provides a procedure for characterizing the performance of field portable fentanyl detection equipment and assays when utilizing the test samples and statistical considerations described in Specification E3243. 1.1.2?This test method descri

Standard Test Method for Establishing Performance of Equipment and Assays for Field Detection of Fentanyl and Fentanyl-Related Compounds

ASTM D6839-21a 多维气相色谱法测定火花点火发动机燃料中碳氢化合物类型、含氧化合物、苯和甲苯的标准试验方法

1.1 This test method covers the quantitative determination of saturates, olefins, aromatics, and oxygenates in sparkignition engine fuels by multidimensional gas chromatography. Each hydrocarbon type can be reported either by carbon number (see Note 1) or as a total. NOTE 1—There can be an overlap between the C9 and C10 aromatics; however, the total is accurate. Isopropyl benzene is resolved from the C8 aromatics and is included with the other C9 aromatics. 1.2 This test method is not intended to determine individual hydrocarbon components except benzene and toluene. 1.3 This test method is divided into two parts, Part A and Part B. 1.3.1 Part A is applicable to the concentration ranges for which precision (Table 10 and Table 11) has been obtained: Property Units Applicable range Total aromatics Volume % 19.32 to 46.29 Total saturates Volume % 26.85 to 79.31 Total olefins Volume % 0.40 to 26.85 Oxygenates Volume % 0.61 to 9.85 Oxygen Content Mass % 2.01 to 12.32 Benzene Volume % 0.38 to 1.98 Toluene Volume % 5.85 to 31.65 Methanol Volume % 1.05 to 16.96 Ethanol Volume % 0.50 to 17.86 MTBE Volume % 0.99 to 15.70 ETBE Volume % 0.99 to 15.49 TAME Volume % 0.99 to 5.92 TAEE Volume % 0.98 to 15.59 1.3.1.1 This test method is specifically developed for the analysis of automotive motor gasoline that contains oxygenates, but it also applies to other hydrocarbon streams having similar boiling ranges, such as naphthas and reformates. 1.3.2 Part B describes the procedure for the analysis of oxygenated groups (ethanol, methanol, ethers, C3 to C5 alcohols) in ethanol fuels containing an ethanol volume fraction between 50 % and 85 % (17 % to 29 % oxygen). The gasoline is diluted with an oxygenate-free component to lower the ethanol content to a value below 20 % before the analysis by GC. The diluting solvent should not be considered in the integration, this makes it possible to report the results of the undiluted sample after normalization to 100 %. 1.4 Oxygenates as specified in Test Method D4815 have been verified not to interfere with hydrocarbons. Within the round robin sample set, the following oxygenates have been tested: MTBE, ethanol, ETBE, TAME, iso-propanol, isobutanol, tert-butanol and methanol. Applicability of this test method has also been verified for the determination of n-propanol, acetone, and di-isopropyl ether (DIPE). However, no precision data have been determined for these compounds. 1.4.1 Other oxygenates can be determined and quantified using Test Method D4815 or D5599. 1.5 The method is harmonized with ISO 22854. 1.6 This test method includes a relative bias section for U.S. EPA spark-ignition engine fuel regulations for total olefins reporting based on Practice D6708 accuracy assessment between Test Method D6839 and Test Method D1319 as a possible Test Method D6839 alternative to Test Method D1319. The Practice D6708 derived correlation equation is only applicable for fuels in the total olefins concentration range from 0.2 % to 18.2 % by volume as measured by Test Method D6839. The applicable Test Method D1319 range for total olefins is from 0.6 % to 20.6 % by volume as reported by Test Method D1319. 1.7 This test method includes a relative bias section for reporting benzene based on Practice D6708 accuracy assessment between Test Method D6839 and Test Method D3606 (Procedure B) as a possible Test Method D6839 alternative to Test Method D3606 (Procedure B). The Practice D6708 derived correlation equation is only applicable for fuels in the benzene concentration range from 0.52 % to 1.67 % by volume as measured by Test Method D6839. 1.8 This test method includes a relative bias section for reporting benzene based on Practice D6708 accuracy assessment between Test Method D6839 and Test Method D5580 as a possible Test Method D6839 alternative to Test Method 1 This test method is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcommittee D02.04.0L on Gas Chromatography Methods. Current edition approved May 1, 2021. Published July 2021. Originally approved in 2002. Last previous edition approved in 2021 as D6839 – 21. DOI: 10.1520/ D6839-21A. *A Summary of Changes section appears at the end of this standard Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 1 D5580. The Practice D6708 derived correlation equation is only applicable for fuels in the benzene concentration range from 0.52 % to 1.67 % by volume as measured by Test Method D6839. 1.9 This test method includes a relative bias section for reporting benzene based on Practice D6708 accuracy assessment between Test Method D6839 and Test Method D5769 as a possible Test Method D6839 alternative to Test Method D5769. The Practice D6708 derived correlation equation is only applicable for fuels in the benzene concentration range from 0.52 % to 1.67 % by volume as measured by Test Method D6839. 1.10 This test method includes a relative bias section for reporting total aromatics based on Practice D6708 accuracy assessment between Test Method D6839 and Test Method D1319 as a possible Test Method D6839 alternative to Test Method D1319. The Practice D6708 derived correlation equation is only applicable for fuels in the total aromatics concentration range from 14.3 % to 31.2 % by volume as measured by Test Method D6839. 1.11 This test method includes a relative bias section for reporting total aromatics based on Practice D6708 accuracy assessment between Test Method D6839 and Test Method D5580 as a possible Test Method D6839 alternative to Test Method D5580. The Practice D6708 derived correlation equation is only applicable for fuels in the total aromatics concentration range from 14.3 % to 31.2 % by volume as measured by Test Method D6839. 1.12 This test method includes a relative bias section for reporting total aromatics based on Practice D6708 accuracy assessment between Test Method D6839 and Test Method D5769 as a possible Test Method D6839 alternative to Test Method D5769. The Practice D6708 derived correlation equation is only applicable for fuels in the total aromatics concentration range from 14.3 % to 30.1 % by volume as measured by Test Method D6839. 1.13 This test method includes a relative bias section for reporting total olefins based on Practice D6708 accuracy assessment between Test Method D6839 and Test Method D6550 as a possible Test Method D6839 alternative to Test Method D6550. The Practice D6708 derived correlation equation is only applicable for fuels in the total olefins concentration range from 1.5 % to 17.2 % by volume as measured by Test Method D6839. 1.14 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.15 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.16 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Test Method for Hydrocarbon Types, Oxygenated Compounds, Benzene, and Toluene in Spark Ignition Engine Fuels by Multidimensional Gas Chromatography

ASTM E3289-21 芬太尼和芬太尼相关化合物现场检测用设备和分析的标准指南

1.1?This guide provides end-users and practitioners with information on the optimal use and limitations of assays and instrumentation designed to detect fentanyl and fentanyl-related compounds. 1.2?This guide also provides summaries and links to guidance documents on training,

Standard Guide for Using Equipment and Assays for Field Detection of Fentanyl and Fentanyl-Related Compounds

ISO 18114:2021 表面化学分析. 次级离子质谱法. 测定离子注入标样中的相对灵敏度系数

This document specifies a method of determining relative sensitivity factors (RSFs) for secondary-ion mass spectrometry (SIMS) from ion-implanted reference materials. The method is applicable to specimens in which the matrix is of uniform chemical composition, and in which the peak concentration of the implanted species does not exceed one atomic percent.

Surface chemical analysis - Secondary-ion mass spectrometry - Determination of relative sensitivity factors from ion-implanted reference materials

21/30433862 DC BS ISO 17109 AMD1 表面化学分析 深度剖析 使用单一和……的 X 射线光电子能谱、俄歇电子能谱和二次离子质谱溅射深度分析中溅射速率测定方法

BS ISO 17109 AMD1. Surface chemical analysis. Depth profiling. Method for sputter rate determination in X-ray photoelectron spectroscopy, Auger electron spectroscopy and secondary-ion mass spectrometry sputter depth profiling using single and…

ASTM E3269-21 测定胶体金悬浮液中颗粒结合金质量分数的标准试验方法

1.1?This test method describes the use of inductively coupled plasma optical emission spectrometry (ICP-OES; also includes ICP-AES, where AES is atomic emission spectrometry) or inductively coupled plasma mass spectrometry (ICP-MS) for the determination of the mass fraction of p

Standard Test Method for Determination of the Mass Fraction of Particle-Bound Gold in Colloidal Gold Suspensions

ISO 20579-3:2021 表面化学分析.样品处理、制备和安装.第3部分：生物材料

This document gives guidance on methods of handling, mounting and surface treatment for a biomaterial specimen prior to surface chemical analysis. It is intended for the analyst as an aid in understanding the specialized specimen-handling conditions required for analyses by the following techniques: — X-ray photoelectron spectroscopy (XPS or ESCA); — secondary ion mass spectrometry (SIMS); — Auger electron spectroscopy (AES). The protocols presented are also applicable to other analytical techniques that are sensitive to surface composition, such as: — attenuated total reflectance -Fourier transform infrared spectroscopy (ATR-FTIR); — total reflection X-ray fluorescence (TXRF); — ultraviolet photoelectron spectroscopy (UPS). The influence of vacuum conditions applied and the issue of contamination before and after analysis and implantation, as well as issues related to contamination during analysis, are addressed. Biomaterials covered here are hard and soft specimens such as metals, ceramics, scaffolds and polymers. This document does not cover such viable biological materials as cells, tissues and living organisms. Other related topics not covered in this document include: preparation of specimens for electron or light microscopy.

Surface chemical analysis - Sample handling, preparation and mounting - Part 3: Biomaterials

BS PD ISO/TR 15969:2021 表面化学分析 深度剖面 溅射深度的测量

Surface chemical analysis. Depth profiling. Measurement of sputtered depth

T/LZZLXH 059-2021 检验检测机构化学分析滴定操作规程

6.3　具塞滴定管的润滑及试漏 6.3.1　涂润滑剂：将滴定管平放，取下旋塞，擦干旋塞和旋塞槽，取少量凡士林（或硅脂），在旋塞孔的细口端（不超过流液孔）及旋塞的粗端（不超过流液孔）沿圆周均匀涂布。将旋塞插入旋塞孔，向同一方向旋转，从外面观察旋塞和旋塞槽整体透明，转动灵活。用橡皮筋固定旋塞。如出现润滑剂堵塞流液孔，可将旋塞及滴定管下端放入热水中使润滑剂融化流出，然后重新涂布。 6.3.2　试漏：用水充满滴定管并将液面调至“0”刻度线，将滴定管夹持在滴定管架上静置约2min，用干燥洁净滤纸检查滴定管下端及旋塞两端不应有液体渗出，观察液面无下降。将活塞旋转180°，再静置约2min再次检查。若漏液，应重新涂润滑剂。 6.4　无塞滴定管的试漏 6.4.1　检查乳胶管是否老化，玻璃珠大小是否合适。 6.4.2　试漏：用水充满滴定管并调至“0”刻度线，将滴定管直立夹持在滴定管架上静置5min。观察液面无下降，滴定管下端无渗出。若有漏水应更换橡皮管或管内玻璃珠，直至不漏水且能灵活控制液滴为止。

Operating procedures for chemical analysis and titration of inspection and testing institutions

T/LZZLXH 062-2021 检验检测机构化学分析移液操作规程

7　移液操作 7.1　单标线吸量管、分度吸量管移液 7.1.1　吸取溶液：用单手的拇指和中指捏住单标线吸量管或分度吸量管的上端，将管的下口插入待吸溶液液面以下适当深度，以不吸入空气为宜，用洗耳球按润洗的吸液方法吸取溶液，当液面升高到刻线以上约5mm时，移去洗耳球，立即用食指堵住上口。 7.1.2　调节液面：将管向上提离液面，用洁净滤纸擦干吸量管外部液体，另取一洁净小烧杯将管竖直，管尖紧贴已倾斜小烧杯内壁，微微松动食指，并轻轻捻转吸量管，使液面平稳下降，直至溶液的弯月面与所要求的标线相切时，立即用食指压紧管口，保持吸量管竖直，移去流液口外最后一滴液体。 7.1.3　放出溶液：使接收容器适当倾斜，吸量管保持竖直，流液口紧靠接收容器内壁，松开食指，让溶液沿器壁自然流出，当液面下降到管尖后，近似等待3s，随即用接收容器内壁移去流液口最后一滴液体，移开吸量管。 7.1.4　标示有“吹”的吸量管应将流液口内的残留液体排出。

Operating procedures for chemical analysis pipetting of inspection and testing institutions

T/CNIA 0120-2021 电子工业用高纯硝酸中痕量杂质元素含量的测定 电感耦合等离子体质谱法

本文件规定了电感耦合等离子体质谱法测定电子工业用高纯硝酸中杂质元素含量（铝、锑、砷、钡、硼、镉、钙、铬、铜、铁、铅、锂、镁、锰、镍、钾、钠、锡、钛、钒、锌）的方法。 本文件适用于电子工业用高纯硝酸中痕量杂质元素含量的测定，各元素测定范围为0.001μg/kg～10.000μg/kg。标准工作曲线法适用于杂质元素含量＞0.100μg/kg～10.000μg/kg；标准加入法适用于杂质元素含量≤0.100μg/kg～0.001μg/kg。

Determination of trace impurity elements in high-purity nitric acid for the electronics industry by inductively coupled plasma mass spectrometry