G04 基础标准与通用方法 标准查询与下载

DB23/T 1451.1-2011 黑龙江省重大危险源辨识分级标准 第1部分：危险化学品

Heilongjiang Province Major Hazard Source Identification and Grading Standard Part 1: Hazardous Chemicals

DB23/T 1449-2011 危险化学品贮罐区、库区和生产场所固定重大危险源监测预警系统建设规范

Specifications for the construction of monitoring and early warning systems for fixed major hazards in storage tank areas, warehouse areas and production sites of hazardous chemicals

NF X21-071:2011 表面化学分析.X射线光电子能谱法.分析用导则

Surface Chemical Analysis - X-ray photoelectron Spectroscopy - Guidelines for analysis.

JIS K 0167:2011 表面化学分析 俄歇电子光谱和X射线光电子能谱学 匀质材料定量分析用实验室测定相对敏感因子的使用指南

Surface chemical analysis -- Auger electron spectroscopy and X-ray photoelectron spectroscopy -- Guide to the use of experimentally determined relative sensitivity factors for the quantitative analysis of homogeneous materials

JIS K 0168:2011 表面化学分析.静态二次离子质谱法用信息格式

Surface chemical analysis -- Information format for static secondary-ion mass spectrometry

JIS K 0050:2011 化学分析一般准则

General rules for chemical analysis

DIN ISO/TS 80004-3:2011 纳米技术.词汇表.第3部分:炭质纳米颗粒(ISO/TS 80004-3-2010)

Nanotechnologies - Vocabulary - Part 3: Carbon nano-objects (ISO/TS 80004-3:2010)

BS DD ISO/TS 25138:2011 表面化学分析.辉光放电发射光谱法分析金属氧化膜

Surface chemical analysis. Analysis of metal oxide films by glow-discharge optical-emission spectrometry

DB51/T 1220-2011 工业用氯片酚含量分析方法

Analytical method for industrial chlorophenes

DB51/T 1221-2011 工业用片酚含量分析方法

Analytical method for industrial flake phenol content

DB51/T 1222-2011 工业用一氯嚬呐酮含量分析方法

Analytical method for the content of monoclonalone for industrial use

ANSI/NSF/GCI 355-2011 绿色化工产品和过程信息标准

Issue 1 - Revision 2: The purpose of this ballot is to create a new standard to provide the chemical enterprise with a voluntary and standardized way to define and report the primary categories of information, their respective data elements, and data quality objectives. This information will be provided by suppliers to communicate clearly, with transparency and consistency, to help customers evaluate the relative greenness of a chemical product and process over its life cycle.

Greener Chemicals and Processes Information Standard

ASTM D6591-11(2017) 采用示差折光检测的高效液相色谱法测定中间馏分中芳香烃类型的标准试验方法

5.1 The aromatic hydrocarbon content of motor diesel fuel is a factor that can affect exhaust emissions and fuel combustion characteristics, as measured by cetane number. 5.2 The United States Environmental Protection Agency (US EPA) regulates the aromatic content of diesel fuels. California Air Resources Board (CARB) regulations place limits on the total aromatics content and polynuclear aromatic hydrocarbon content of motor diesel fuel, thus requiring an appropriate analytical determination to ensure compliance with the regulations. 5.3 This test method is applicable to materials in the same boiling range as motor diesel fuels and is unaffected by fuel coloration. Test Method D1319, which has been mandated by the US EPA for the determination of aromatics in motor diesel fuel, excludes materials with final boiling points greater than 3158201;°C (6008201;°F) from its scope. Test Method D2425 is applicable to the determination of both total aromatics and polynuclear aromatic hydrocarbons in diesel fuel, but is much more costly and time-consuming to perform. Test Method D5186, currently specified by CARB, is also applicable to the determination of both total aromatics and polynuclear aromatic hydrocarbons in diesel fuel. Test Method D5186, however, specifies the use of supercritical fluid chromatography equipment that may not be readily available. Note 2: Test Method D5186 was previously specified by CARB as an alternative to Test Method D1319. 1.1 This test method covers a high performance liquid chromatographic test method for the determination of mono-aromatic, di-aromatic, tri+-aromatic, and polycyclic aromatic hydrocarbon contents in diesel fuels and petroleum distillates boiling in the range from 1508201;°C to 4008201;°C. The total aromatic content in % m/m is calculated from the sum of the corresponding individual aromatic hydrocarbon types. Note 1: Aviation fuels and petroleum distillates with a boiling point range from 508201;°C to 3008201;°C are not determined by this test method and should be analyzed by Test Method, D6379 or other suitable equivalent test methods. 1.2 The precision of this test method has been established for diesel fuels and their blending components, containing from 48201;% to 408201;% (m/m) mono-aromatic hydrocarbons, 08201;% to 208201;% (m/m) di-aromatic hydrocarbons, 08201;% to 68201;% (m/m) tri+-aromatic hydrocarbons, 08201;% to 26 % (m/m) polycyclic aromatic hydrocarbons, and 48201;% to 658201;% (m/m) total aromatic hydrocarbons. 1.3 Compounds containing sulfur, nitrogen, and oxygen are possible interferents. Mono-alkenes do not interfere, but conjugated di- and poly-alkenes, if present, are possible interferents.

Standard Test Method for Determination of Aromatic Hydrocarbon Types in Middle Distillates&x2014;High Performance Liquid Chromatography Method with Refractive Index Detection

ASTM E135-11b 与金属、矿石和相关材料用分析化学相关的标准术语

Definitions given in Section 4 are intended for use in all standards on analytical chemistry for metals, ores, and related materials. The definitions should be used uniformly and consistently. The purpose of this terminology is to promote clear understanding and interpretation of the standards in which definitions are used.1.1 This is a compilation of terms commonly used in analytical chemistry for metals, ores, and related materials. Terms that are generally understood or defined adequately in other readily available sources are either not included or their sources are identified. 1.2 A definition is a single sentence with additional information included in a discussion. 1.3 Definitions identical to those published by another standards organization or ASTM committee are identified with the name of the organization or the identifying document and ASTM committee. 1.4 Definitions specific to a particular field (such as emission spectrometry) are identified with an italicized introductory phrase.

Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials

ASTM D6591-11 用带检测折光指数的高效液相色谱法测定中间馏分中芳香烃类型的标准试验方法

The aromatic hydrocarbon content of motor diesel fuel is a factor that can affect exhaust emissions and fuel combustion characteristics, as measured by cetane number. The United States Environmental Protection Agency (US EPA) regulates the aromatic content of diesel fuels. California Air Resources Board (CARB) regulations place limits on the total aromatics content and polynuclear aromatic hydrocarbon content of motor diesel fuel, thus requiring an appropriate analytical determination to ensure compliance with the regulations. This test method is applicable to materials in the same boiling range as motor diesel fuels and is unaffected by fuel coloration. Test Method D1319, which has been mandated by the US EPA for the determination of aromatics in motor diesel fuel, excludes materials with final boiling points greater than 315°C (600°F) from its scope. Test Method D2425 is applicable to the determination of both total aromatics and polynuclear aromatic hydrocarbons in diesel fuel, but is much more costly and time-consuming to perform. Test Method D5186, currently specified by CARB, is also applicable to the determination of both total aromatics and polynuclear aromatic hydrocarbons in diesel fuel. Test Method D5186, however, specifies the use of supercritical fluid chromatography equipment that may not be readily available. Note 28212;Test Method D5186 was previously specified by CARB as an alternative to Test Method D1319.1.1 This test method covers a high performance liquid chromatographic test method for the determination of mono-aromatic, di-aromatic, tri+-aromatic, and polycyclic aromatic hydrocarbon contents in diesel fuels and petroleum distillates boiling in the range from 150 to 400°C. The total aromatic content in % m/m is calculated from the sum of the corresponding individual aromatic hydrocarbon types. Note 18212;Aviation fuels and petroleum distillates with a boiling point range from 50 to 300°C are not determined by this test method and should be analyzed by Test Method, D6379 or other suitable equivalent test methods. 1.2 The precision of this test method has been established for diesel fuels and their blending components, containing from 4 to 40 % (m/m) mono-aromatic hydrocarbons, 0 to 20 % (m/m) di-aromatic hydrocarbons, 0 to 6 % (m/m) tri+-aromatic hydrocarbons, 0 to 26 % (m/m) polycyclic aromatic hydrocarbons, and 4 to 65 % (m/m) total aromatic hydrocarbons. 1.3 Compounds containing sulfur, nitrogen, and oxygen are possible interferents. Mono-alkenes do not interfere, but conjugated di- and poly-alkenes, if present, are possible interferents. 1.4 By convention, this standard defines the aromatic hydrocarbon types on the basis of their elution characteristics from the specified liquid chromatography column relative to model aromatic compounds. Quantification is by external calibration using a single aromatic compound, which may or may not be representative of the aromatics in the sample, for each aromatic hydrocarbon type. Alternative tec......

Standard Test Method for Determination of Aromatic Hydrocarbon Types in Middle Distillatesmdash;High Performance Liquid Chromatography Method with Refractive Index Detection

ASTM D7169-11 用高温气相色谱法对含有诸如原油, 大气和真空残留物的试样沸点分布的标准试验方法

The determination of the boiling point distribution of crude oils and vacuum residues, as well as other petroleum fractions, yields important information for refinery operation. These boiling point distributions provide information as to the potential mass percent yield of products. This test method may provide useful information that can aid in establishing operational conditions in the refinery. Knowledge of the amount of residue produced is important in determining the economics of the refining process.1.1 This test method covers the determination of the boiling point distribution and cut point intervals of crude oils and residues by using high temperature gas chromatography. The amount of residue (or sample recovery) is determined using an external standard. 1.2 This test method extends the applicability of simulated distillation to samples that do not elute completely from the chromatographic system. This test method is used to determine the boiling point distribution through a temperature of 720°C. This temperature corresponds to the elution of n-C100. 1.3 This test method is used for the determination of boiling point distribution of crude oils. This test method uses capillary columns with thin films, which results in the incomplete separation of C4-C8 in the presence of large amounts of carbon disulfide, and thus yields an unreliable boiling point distribution corresponding to this elution interval. In addition, quenching of the response of the detector employed to hydrocarbons eluting during carbon disulfide elution, results in unreliable quantitative analysis of the boiling distribution in the C4-C8 region. Since the detector does not quantitatively measure the carbon disulfide, its subtraction from the sample using a solvent-only injection and corrections to this region via quenching factors, results in an approximate determination of the net chromatographic area. A separate, higher resolution gas chromatograph (GC) analysis of the light end portion of the sample may be necessary in order to obtain a more accurate description of the boiling point curve in the interval in question (see Appendix X1). 1.4 This test method is also designed to obtain the boiling point distribution of other incompletely eluting samples such as atmospheric residues, vacuum residues, etc., that are characterized by the fact that the sample components are resolved from the solvent. 1.5 This test method is not applicable for the analysis of materials containing a heterogeneous component such as polyesters and polyolefins. 1.6 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard. 1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in Section 8.

Standard Test Method for Boiling Point Distribution of Samples with Residues Such as Crude Oils and Atmospheric and Vacuum Residues by High Temperature Gas Chromatography

ASTM D4739-11 电势滴定法测定碱值的标准试验方法

New and used petroleum products can contain basic constituents that are present as additives. The relative amount of these materials can be determined by titration with acids. The base number is a measure of the amount of basic substances in the oil always under the conditions of the test. It is sometimes used as a measure of lubricant degradation in service. However, any condemning limit shall be empirically established. 5.2 As stated in 1.2, this test method uses a weaker acid to titrate the base than Test Method D2896, and the titration solvents are also different. Test Method D2896 uses a stronger acid and a more polar solvent system than Test Method D4739. As a result, Test Method D2896 will titrate salts of weak acids (soaps), basic salts of polyacidic bases, and weak alkaline salts of some metals. They do not protect the oil from acidic components due to the degradation of the oil. This test method may produce a falsely exaggerated base number. Test Method D4739 will probably not titrate these weak bases but, if so, will titrate them to a lesser degree of completion. It measures only the basic components of the additive package that neutralizes acids. On the other hand, if the additive package contains weak basic components that do not play a role in neutralizing the acidic components of the degrading oil, then the Test Method D4739 result may be falsely understated. 5.3 Particular care is required in the interpretation of the base number of new and used lubricants. 5.3.1 When the base number of the new oil is required as an expression of its manufactured quality, Test Method D2896 is preferred, since it is known to titrate weak bases that this test method may or may not titrate reliably. 5.3.2 When the base number of in-service or at-term oil is required, this test method is preferred because in many cases, especially for internal combustion engine oils, weakly basic degradation products are possible. Test Method D2896 will titrate these, thus giving a false value of essential basicity. This test method may or may not titrate these weak acids. 5.3.3 When the loss of base number value, as the oils proceed in service, is the consideration, this test method is to be preferred and all values including the unused oil shall be determined by this test method. Base numbers obtained by this test method shall not be related to base numbers obtained by another test method such as Test Method D2896. 5.3.4 In ASTM Interlaboratory Crosscheck Programs for both new and used lubricants, historically Test Method D2896 gives a higher value for base number.1.1 This test method covers a procedure for the determination of basic constituents in petroleum products and new and used lubricants. This test method resolves these constituents into groups having weak-base and strong-base ionization properties, provided the dissociation constants of the more strongly basic compounds are at least 1000 times than that of the next weaker groups. This test method covers base numbers up to 250. 1.2 In new and used lubricants, the constituents that can be considered to have basic properties are primarily organic and inorganic bases, including amino compounds. This test method uses hydrochloric acid as the titrant, whereas Test Method

Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration

ASTM UOP683-11 炼油废水中的硫化物

This method is for determining the sulfide content in refinery waste water using cadmium chloride. The range of quantitation is from 1 mg/kg (mass-ppm) to 2 mass-% as sulfur. It is not applicable to caustic solutions. If present, polysulfides may interfere with the analysis.

Sulfide in Refinery Waste Water

ASTM D974-11 用颜色指示剂滴定法测定酸碱值的标准试验方法

New and used petroleum products can contain basic or acidic constituents that are present as additives or as degradation products formed during service, such as oxidation products. The relative amount of these materials can be determined by titrating with acids or bases. This number, whether expressed as acid number or base number, is a measure of this amount of acidic or basic substances, respectively, in the oilalways under the conditions of the test. This number is used as a guide in the quality control of lubricating oil formulations. It is also sometimes used as a measure of lubricant degradation in service; however, any condemning limits must be empirically established. Since a variety of oxidation products contribute to the acid number and the organic acids vary widely in corrosive properties, the test cannot be used to predict corrosiveness of an oil under service conditions. No general correlation is known between acid number and the corrosive tendency of oils toward metals. Compounded engine oils can and usually do have both acid and base numbers in this test method.1.1 This test method covers the determination of acidic or basic constituents (Note 1) in petroleum products and lubricants soluble or nearly soluble in mixtures of toluene and isopropyl alcohol. It is applicable for the determination of acids or bases whose dissociation constants in water are larger than 10−9; extremely weak acids or bases whose dissociation constants are smaller than 10−9 do not interfere. Salts react if their hydrolysis constants are larger than 10−9. Note 18212;In new and used oils, the constituents considered to have acidic characteristics include organic and inorganic acids, esters, phenolic compounds, lactones, resins, salts of heavy metals, and addition agents such as inhibitors and detergents. Similarly, constituents considered to have basic properties include organic and inorganic bases, amino compounds, salts of weak acids (soaps), basic salts of polyacidic bases, salts of heavy metals, and addition agents such as inhibitors and detergents. Note 28212;This test method is not suitable for measuring the basic constituents of many basic additive-type lubricating oils. Test Method D4739 can be used for this purpose. 1.2 This test method can be used to indicate relative changes that occur in an oil during use under oxidizing conditions. Although the titration is made under definite equilibrium conditions, the method does not measure an absolute acidic or basic property that can be used to predict performance of an oil under service conditions. No general relationship between bearing corrosion and acid or base numbers is known. Note 38212;Oils, such as many cutting oils, rustproofing oils, and similar compounded oils, or excessively dark-colored oils, that cannot be analyzed for acid number by this test method due to obscurity of the color-indicator end point, can be analyzed by Test Method D664. The acid numbers obtained by this color-indicator test method need not be numerically the same as those obtained by Test Method D664, the base numbers obtained by this color indicator test method need not be numerically the same as those obtained by Test Method

Standard Test Method for Acid and Base Number by Color-Indicator Titration

ASTM D4739-11(2017) 采用盐酸电位滴定法测定碱值的标准试验方法

5.1 New and used petroleum products can contain basic constituents that are present as additives. The relative amount of these materials can be determined by titration with acids. The base number is a measure of the amount of basic substances in the oil always under the conditions of the test. It is sometimes used as a measure of lubricant degradation in service. However, any condemning limit shall be empirically established. 5.2 As stated in 1.2, this test method uses a weaker acid to titrate the base than Test Method D2896, and the titration solvents are also different. Test Method D2896 uses a stronger acid and a more polar solvent system than Test Method D4739. As a result, Test Method D2896 will titrate salts of weak acids (soaps), basic salts of polyacidic bases, and weak alkaline salts of some metals. They do not protect the oil from acidic components due to the degradation of the oil. This test method may produce a falsely exaggerated base number. Test Method D4739 will probably not titrate these weak bases but, if so, will titrate them to a lesser degree of completion. It measures only the basic components of the additive package that neutralizes acids. On the other hand, if the additive package contains weak basic components that do not play a role in neutralizing the acidic components of the degrading oil, then the Test Method D4739 result may be falsely understated. 5.3 Particular care is required in the interpretation of the base number of new and used lubricants. 5.3.1 When the base number of the new oil is required as an expression of its manufactured quality, Test Method D2896 is preferred, since it is known to titrate weak bases that this test method may or may not titrate reliably. 5.3.2 When the base number of in-service or at-term oil is required, this test method is preferred because in many cases, especially for internal combustion engine oils, weakly basic degradation products are possible. Test Method D2896 will titrate these, thus giving a false value of essential basicity. This test method may or may not titrate these weak acids. 5.3.3 When the loss of base number value, as the oils proceed in service, is the consideration, this test method is to be preferred and all values including the unused oil shall be determined by this test method. Base numbers obtained by this test method shall not be related to base numbers obtained by another test method such as Test Method D2896. 5.3.4 In ASTM Interlaboratory Crosscheck Programs for both new and used lubricants, historically Test Method D2896 gives a higher value for base number. 1.1 This test method covers a procedure for the determination of basic constituents in petroleum products and new and used lubricants. This test method resolves these co......

Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration