BS PD CEN/TR 15641-2007
食品分析.液相色谱串联质谱法测定农药残留物.串联质谱测定参数已作废

Food analysis — Determination of pesticide residues by LC-MS/MS — Tandem mass spectrometric parameters

BS PD CEN/TR 15641-2007 发布历史

Standards for the determination of pesticide residues in foods of plant origin that use LC-MS/MS, such as the standards in preparation: prEN 15637 "Foods of plant origin — Determination of pesticide residues using LC-MS/MS following methanol extraction and clean up using diatomaceous earth" prEN 15662 "Foods of plant origin — Determination of pesticide residues using GC-MS and/or LC-MS/MS following acetonitrile extraction/partitioning by dispersive SPE — QuEChERS-method” To facilitate the determination of active substances and/or metabolites using LC-MS/MS, Table 1 specifies the precursor ions and product ions suitable for quantification, which can be used independently of the type of triple quadrupole mass spectrometer. However, using an ion trap mass spectrometer other product ions can be generated or at least the relative intensities of the ions are different to triple quadrupole instruments. Furthermore, the additional parameters declustering potential (DP), collision energy (CE), relative retention times and an approximate classification of detection sensitivity are presented in Table 1. These were derived using the API 20001) and should be applicable at least for other instruments of the API type (Applied Biosystems).

BS PD CEN/TR 15641-2007由英国标准学会 GB-BSI 发布于 2007-09-28，于 2007-09-28 废止。

BS PD CEN/TR 15641-2007 在中国标准分类中归属于: X04 基础标准与通用方法。

BS PD CEN/TR 15641-2007的历代版本如下：

• 2007年09月28日 BS PD CEN/TR 15641-2007 食品分析.液相色谱串联质谱法测定农药残留物.串联质谱测定参数

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标准号

BS PD CEN/TR 15641-2007

发布日期

2007年09月28日

实施日期

废止日期

2007-09-28

中国标准分类号

X04

发布单位

GB-BSI

适用范围

Standards for the determination of pesticide residues in foods of plant origin that use LC-MS/MS, such as the standards in preparation: prEN 15637 "Foods of plant origin — Determination of pesticide residues using LC-MS/MS following methanol extraction and clean up using diatomaceous earth" prEN 15662 "Foods of plant origin — Determination of pesticide residues using GC-MS and/or LC-MS/MS following acetonitrile extraction/partitioning by dispersive SPE — QuEChERS-method” To facilitate the determination of active substances and/or metabolites using LC-MS/MS, Table 1 specifies the precursor ions and product ions suitable for quantification, which can be used independently of the type of triple quadrupole mass spectrometer. However, using an ion trap mass spectrometer other product ions can be generated or at least the relative intensities of the ions are different to triple quadrupole instruments. Furthermore, the additional parameters declustering potential (DP), collision energy (CE), relative retention times and an approximate classification of detection sensitivity are presented in Table 1. These were derived using the API 20001) and should be applicable at least for other instruments of the API type (Applied Biosystems).

BS PD CEN/TR 15641-2007 中可能用到的仪器设备