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5.1x00a0;Viscosityx2014;Viscosity values determined by this test method depend on molecular structure, molecular weight, and non-rubber constituents that may be present. Since rubber behaves as a non-Newtonian fluid, no simple relationship exists between the molecular weight and the viscosity. Therefore, caution must be exercised in interpreting viscosity values of rubber, particularly in cases where molecular weight is very high. For example, as the molecular weight increases, the viscosity values for IIR polymers (butyl rubbers) reach an upper limit of about 80, at 100x00b0;C (212x00b0;F) using a large rotor at a rotation speed of 2 r/min, and may then decrease to considerably lower values. For these higher molecular weight rubbers, better correlation between viscosity values and molecular weight is obtained if the test temperature is increased.
5.2x00a0;Stress Relaxationx2014;The stress relaxation behavior of rubber is a combination of both an elastic and a viscous response. Viscosity and stress relaxation behavior do not depend on such factors as molecular weight and non-rubber constituents in the same way. Thus both of these tests are important and complement each other. A slow rate of relaxation indicates a higher elastic component in the overall response, while a rapid rate of relaxation indicates a higher viscous component. The rate of stress relaxation has been found to correlate with rubber structure characteristics such as molecular weight distribution, chain branching, and gel content.
5.3x00a0;Pre-Vulcanization Characteristicsx2014;The onset of vulcanization can be detected with the Mooney viscometer as evidenced by an increase in viscosity. Therefore, this test method can be used to measure incipient cure (scorch) time and the rate of cure during very early stages of vulcanization. This test method cannot be used to study complete vulcanization because the continuous rotation of the disk will result in slippage when the specimen reaches a stiff consistency.
1.1x00a0;These test methods cover procedures for measuring a property called Mooney viscosity. Mooney viscosity is defined as the shearing torque resisting rotation of a cylindrical metal disk (or rotor) embedded in rubber within a cylindrical cavity. The dimensions of the shearing disk viscometer, test temperatures, and procedures for determining Mooney viscosity are defined in these test methods.
1.2x00a0;When disk rotation is abruptly stopped, the torque or stress on the rotor decreases at some rate depending on the rubber being tested and the temperature of the test. This is called x201c;stress relaxationx201d; and these test methods describe a test method for measuring this relaxation.
Note 1:x00a0;Viscosity as used in these test methods is not a true viscosity and should be interpreted to mean Mooney viscosity, a measure of shearing torque averaged over a range of shearing rates. Stress relaxation is also a function of the test configuration and for these test methods the results are unique to the Mooney viscometer.
1.3x00a0;When compounded rubber is placed in the Mooney viscometer at a temperature at which vulcan......
门尼粘度计是用来测定生胶或混炼胶之门尼粘度的仪器,提供了三种测定数据,一是门尼粘度的测定,二为应力松弛特性的测定,三为焦烧时间的测定。 硫变仪是橡胶行业用来控制质量,快速检验及橡胶基础研究应用最广泛的仪器,为橡胶最优化配方组合提供了精确的数据,可精确测出焦烧时间、正硫化时间、硫化指数及最大、最小转矩等参数。硫化仪采用计算机控制,在计算机上设定好参数后直接控制硫化仪的试验参数。...
门尼焦烧的试验原理 用门尼粘度仪测定胶料焦烧是在特定的条件下, 根据未硫化胶料门尼粘度的变化,测定橡胶开始出现硫化现象的时间。 橡胶硫化特性测定 为了测定橡胶硫化程度及橡胶硫化过程过去采用方法有化学法(结合硫法、溶胀法),物理机械性能法(定伸应力法、拉伸强度法、永久变形法等),这些方法存在的主要缺点是不能连续测定硫化过程的全貌。...
门尼粘度计,门尼粘度仪,橡胶门尼仪用于胶料粘度和硫化指数的测定。在规定的温度下,混合橡胶放在上下平板膜腔之间并施以正弦波扭矩振动时,随着橡胶的硫化测定其扭矩的变化。可根据zui大扭矩、zui小扭矩、焦烧时间、硫化时间、粘弹性等其它因素的变化求出硫化特性的试验机。硫化是橡胶制品制造工艺中zui重要的工艺过程之一。就是使橡胶大分子链由线性变为网状的交联过程,从而获得良好物理机械性能和化学性能。...
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