IEC/TR 62697-2-2018
从未使用和已使用绝缘油中腐蚀性硫化物定量测定试验方法.第2部分:总腐蚀硫（TCS）定量测定的试验方法

Test methods for quantitative determination of corrosive sulfur compounds in unused and used insulating liquids - Part 2: Test method for quantitative determination of total corrosive sulfur (TCS)

IEC/TR 62697-2-2018 发布历史

This part of IEC 62697 specifies a test method for the quantitative determination of total corrosive sulfur (TCS) in unused and used insulating liquids and solid matrices through the conversion of corrosive sulfur species to metal (copper, silver etc.) sulfides. The sulfides formed are quantitatively converted to sulfates; sulfates are determined through turbidity measurement or with ion chromatography. The method is applicable with the following matrices: a) Unused and used insulating liquids, for example mineral insulating oils and natural esters, which allow the determination of corrosive sulfur compounds over concentrations ranging between 2,5 mg kg-1 to 80 mg kg-1 TCS. b) Solid matrices that come in contact with the insulating liquid, for example insulating papers in electrical equipment. The quantification limits for these matrices depend on the amount of matrix used during the determination. The method can be used for the quantitative or semi-quantitative determination of copper sulfide on paper after the test according to IEC 62535. The method can provide unambiguous quantitative assessment of copper sulfide present on paper rather than qualitative results obtained with the SEM-EDX examination stipulated in case of doubts in the interpretation of results obtained from the inspection of paper according to IEC 62535:2008, 6.3. c) Paper and other solid insulating material/s obtained from failed transformers, reactors and other electrical equipment to assist in failure diagnostics. d) Metal deactivator or passivators additives present in insulating liquids (qualitative assessment). However, the method is not applicable for assessing corrosion phenomena for example the dissolution of copper in insulating liquids and deposition on solid matrices, which do not lead to sulfide formation.

IEC/TR 62697-2-2018由国际电工委员会 IX-IEC 发布于 2018-0201。

IEC/TR 62697-2-2018 在中国标准分类中归属于: E38 绝缘油，在国际标准分类中归属于: 29.040.10 绝缘油。

IEC/TR 62697-2-2018 发布之时，引用了标准

• IEC 62697-1-2012 从未使用和已使用绝缘油中腐蚀性硫化物定量测定试验方法.第1部分:二苄二硫(DBDS)定量测定试验方法*， 2012-08-01 更新

* 在 IEC/TR 62697-2-2018 发布之后有更新，请注意新发布标准的变化。

IEC/TR 62697-2-2018的历代版本如下：

• 1970年01月 IEC/TR 62697-2-2018 从未使用和已使用绝缘油中腐蚀性硫化物定量测定试验方法.第2部分:总腐蚀硫（TCS）定量测定的试验方法

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标准号

IEC/TR 62697-2-2018

发布日期

1970年01月

实施日期

废止日期

无

中国标准分类号

E38

国际标准分类号

29.040.10

发布单位

IX-IEC

引用标准

IEC 62697-1-2012

被代替标准

IEC 10/1013/DTR-2017

适用范围

This part of IEC 62697 specifies a test method for the quantitative determination of total corrosive sulfur (TCS) in unused and used insulating liquids and solid matrices through the conversion of corrosive sulfur species to metal (copper, silver etc.) sulfides. The sulfides formed are quantitatively converted to sulfates; sulfates are determined through turbidity measurement or with ion chromatography. The method is applicable with the following matrices: a) Unused and used insulating liquids, for example mineral insulating oils and natural esters, which allow the determination of corrosive sulfur compounds over concentrations ranging between 2,5 mg kg-1 to 80 mg kg-1 TCS. b) Solid matrices that come in contact with the insulating liquid, for example insulating papers in electrical equipment. The quantification limits for these matrices depend on the amount of matrix used during the determination. The method can be used for the quantitative or semi-quantitative determination of copper sulfide on paper after the test according to IEC 62535. The method can provide unambiguous quantitative assessment of copper sulfide present on paper rather than qualitative results obtained with the SEM-EDX examination stipulated in case of doubts in the interpretation of results obtained from the inspection of paper according to IEC 62535:2008, 6.3. c) Paper and other solid insulating material/s obtained from failed transformers, reactors and other electrical equipment to assist in failure diagnostics. d) Metal deactivator or passivators additives present in insulating liquids (qualitative assessment). However, the method is not applicable for assessing corrosion phenomena for example the dissolution of copper in insulating liquids and deposition on solid matrices, which do not lead to sulfide formation.

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