Gatan 695.C/PIPS II 系统离子减薄仪 技术特点

【技术特点】-- Gatan 695.C/PIPS II 系统离子减薄仪

仪器介绍：

名称：离子减薄仪

品牌：美国Gatan

型号：695

技术参数：

离子源
离子枪 两个潘宁离子枪与微型稀土永磁体
减薄角度 +10° 到 -10°，每个离子枪均独立可调节
离子束能量 100eV 到6.0 KeV
光束直径 5keV 下350μm FWHM - 宽离子枪5keV 下800μm FWHM
离子电流密度 最大 10mA/cm2
离子束调制 通过荧光屏精密调整离子束
离子束尺寸 通过气体控制调整
真空
干燥泵系统 两个部分，隔膜机械泵搭配一个70 升/秒涡轮分子泵
压力 5E-6 Torr（6.6E-4Pa）基本压力
8E-5 Torr（10.7E-3Pa）工作压力
真空计 样品室冷阴极标尺，搭配固态压力传感器
样品调换 Gatanzl WhisperlokTM，样品更换时间＜1分钟
样品的Airlock <30 秒
功率
能量消耗 运行时需200W，离子枪关闭时需100W
电源要求 通用电压 100VAC-240VAC，50/60Hz（用户需确定电压和频率）
气体 氩气 25psi （1.42 bar,0.18 MPa）

优点

• 使用 X、Y 样品台来把减薄区域精确定位到离子束交叉点

• 改进低电压性能的离子枪，有用电压低至 100 伏，从而快速安全地对 FIB 制备的TEM样品进行抛光

• 利用 DigitalMicrograph® 软件和光学数码显微镜进行图像存储和分析

• 10 英寸彩色触摸屏可用于显示和控制所有 PIPS™ II 参数

【技术特点对用户带来的好处】-- Gatan 695.C/PIPS II 系统离子减薄仪

【典型应用举例】-- Gatan 695.C/PIPS II 系统离子减薄仪

【产品所获奖项】-- Gatan 695.C/PIPS II 系统离子减薄仪

出版物

Comparison of preparation techniques for nuclear materials for transmission electron microscopy (TEM)

Journal of Nuclear Materials

2015

Aitkaliyeva, A.; Madden, J. W.; Miller, B. D.; Cole, J. I.; Gan, J.

Effect of supersonic fine particle bombardment on microstructure and fatigue properties of Ti-6.5 Al-3.5 Mo-1.5 Zr-0.3 Si titanium alloy at different temperatures

Surface and Coatings Technology

2021

Wu, Y.; Xiong, Y.; Liu, W.; Chen, Z.; Zhang, X.; Wang, S.; Cao, W.

Effect of aging time on the microstructural characterization and corrosion resistance of Al-4.5 Cu-1Li-0.4 Mg-0.4 Ag-0.4 Mn-0.5 Zn alloys

International Journal of Metallurgy and Metal Physics

2021

Chen, W.; Ding, D.; Zhang, W.; Xiao, D.

Thickness and defocus dependence of inter-atomic electric fields measured by scanning diffraction

Ultramicroscopy

2020

Addiego, C.; Gao, W.; Pan, X.

Correlation of threading dislocations with the electron concentration and mobility in InN heteroepitaxial layers grown by MBE

ECS Journal of Solid State Science and Technology

2019

Adikimenakis, A.; Chatzopoulou, P.; Dimitrakopulos, G. P.; Kehagias, Th.; Tsagaraki, K.; Androulidaki, M.; Doundoulakis, G.; Kuzmik, J.; Georgakilas, A.

Identification of interstratified mica and pyrophyllite monolayers within chlorite using advanced scanning/transmission electron microscopy

American Mineralogist

2019

Wang, G.; Wang, H.; Wen, J.

Optimization of mechanical and corrosion properties of plasma sprayed low-chromium containing Fe-based amorphous/nanocrystalline composite coating

Surface and Coatings Technology

2019

Kumar, A.; Nayak, S. K.; Bijalwan, P.; Dutta, M.; Banerjee, A.; Laha, T.

Effects of substrate and post‐deposition annealing on structural and optical properties of (ZnO)1−x(GaN)x films

Basic Solid State Physics

2019

Olsen, V. S.; Bazioti, C.; Baldissera, G.; Azarov, A.; Prytz, Ø.; Persson, C.; Svensson, B. G.; Kuznetsov, A. Y.; Vines, L.

Continuous polycrystalline silicon layers on glass grown from tin solutions

CrystEngComm

2016

Bansen, R.; Ehlers, C.; Teubner, T.; Markurt, T.; Schmidtbauer, J.; Boeck, T.

Interface morphology and composition of Ga(NAsP) quantum well structures for monolithically integrated LASERs on silicon substrates

Journal of Physics D: Applied Physics

2016

Wegele, T.; Beyer, A.; Ludewig, P.; Rosenow, P.; Duschek, L.; Jandieri, K.; Tonner, R.; Stolz, W.; Volz, K.

Assessment of residual stress fields at deformation twin tips and the surrounding environments

Acta Materialia

2016

Abdolvand, H.; Wilkinson, A. J.

Effects of texture and grain size on mechanical properties of AZ80 magnesium alloys at lower temperatures

Materials & Design

2016

Wang, L.; Mostaed, E.; Cao, X.; Huang, G.; Fabrizi, A.; Bonollo, F.; Chi, C.; Vedani, M.

Cross-sectional transmission electron microscopy specimen preparation technique by backside Ar ion milling

Applied Microscopy

2015

Yoo, J. H.; Yang, J. -M.

Microstructure and wear properties of Fe–6wt.%Cr–0.55wt.%C–Xwt.%Nb laser cladding coating and the mechanism analysis

Materials & Design

2015

Yang, J.; Huang, J.; Fan, D.; Chen, S.

On the benefit of aberration-corrected HAADF-STEM for strain determination and its application to tailoring ferroelectric domain patterns

Ultramicroscopy

2015

Tang, Y. L.; Zhu, Y. L.; Ma, X. L.

Evolution of annealing texture in cryo-rolled copper

Materials Science and Engineering: A

2015

Anand, G.; Barai, K.; Madhavan, R. Chattopadhyay, P. P.

Thermodynamic modelling of Al-UX (X= Si, Zr)

Journal of Nuclear Materials

2015

Rabin, D.; Shneck, R. Z.; Rafailov, G.; Dahan, I.; Meshi, L.; Brosh, E.

Local structure and thermoelectric properties of Mg 2 Si 0.977-x Ge x Bi 0.023

Journal of Alloys and Compounds

2015

Farahi, N.; Prabhudev, S.; Botton, G. A.; Zhao, J.; Tse, J. S.; Liu, Z.; Salvador, J. R.; Kleink, H.

Microstructural evolution of nanometric Ti(NiCu)2 precipitates in annealed Ni–Ti–Cu thin films

Vacuum

2015

Callisti, M.; Polcar, T.

The hardness and related deformation mechanisms in nanoscale crystalline–amorphous multilayers

Thin Solid Films

2015

Cui, Y.; Huang, P.; Wang, F.; Lu, T. J.; Xu, K. W.

Quantification of ordering at a solid-liquid interface using plasmon electron energy loss spectroscopy

Applied Physics Letters

2015

Gandman, M.; Kauffmann, Y.; Kaplan, W. D.

Identification of densification mechanisms of pressure-assisted sintering: application to hot pressing and spark plasma sintering of alumina

Journal of Materials Science

2014

Antou, G.; Guyot, P.; Pradeilles, N.; Vandenhende, M.; Maître, A.

Structural evolution and strain induced mixing in Cu-Co composites studied by transmission electron microscopy and atom probe tomography

Materials Characterization

2014

Bachmaier, A.; Aboulfadl, H.; Pfaff, M.; Mücklich, F.; Motz, C.

Investigation of the microstructure and the influence of iron on the formation of Al8Mn5 particles in twin roll cast AZ31 magnesium alloy

Journal of Alloys and Compounds

2014

Pawar, S.; Zhou, X.; Hashimoto, T.; Thompson, G. E.; Scamans, G.; Fan, Z.

Materials News: Interfacial chemistry and atomic arrangement of ZrO2 − La2/3Sr1/3MnO3 pillar-matrix structures

APL Materials

2014

Zhou, D.; Sigle, W.; Okunishi, E.; Wang, Y.; Kelsch, M.; Habermeier, H. -U.; van Aken, P. A.

Microstructure characteristics of high lift factor MOCVD REBCO coated conductors with high Zr content

IEEE Transactions on Applied Superconductivity

2014

Galstyan, E.; Gharacheshmeh, H. M.; Delgado, L.; Xu, A.; Majkic, G.; Selvamanickam, V.

Automated CBED processing: Sample thickness estimation based on analysis of zone-axis CBED pattern

Ultramicroscopy

2014

Klinger, M.; Němec, M.; Polívka, L.; Gärtnerová, V.; Jäger, A.

Anomalous deformation twinning in coarse-grained Cu in Ag60Cu40 composites under high strain-rate compressive loading

Materials Science and Engineering: A

2014

Eftink, B. P.; Mara, N. A.; Kingstedt, O. T.; Safarik, D. J.; Lambros, J.; Robertson, I. M.

A study of one-dimensional incommensurate modulated structure determination in high-resolution transmission electron microscopy

Foundations of Crystallography

2014

Li, X.; Ge, B.; Li, F.; Luo, H.; Wen, H.

Effect of wavelength modulation of arc evaporated Ti–Al–N/Ti–Al–V–N multilayer coatings on microstructure and mechanical/tribological properties

Thin Solid Films

2014

Pfeiler-Deutschmann, M.; Mayrhofer, P. H.; Chladil, K.; Penoy, M.; Michotte, C.; Kathrein, M.; Mitterer, C.

Investigation of deformations and strain fields in silicon matrix structures embedded with vertically stacked Ge(Si) self-assembled islands

Applied Physics Letters

2014

Pavlov, D. A.; Bobrov, A. I.; Novikov, A. V.; Sorokin, D. S.; Malekhonova, N. V.; Pirogov, A. V.; Nikolitchev, D. E.; Boryakov, A. V.

Growth of InAs/GaAs quantum dots covered by GaAsSb in multiple structures studied by reflectance anisotropy spectroscopy

Journal of Crystal Growth

2014

Hospodková, A.; Pangrác, J.; Vyskočil, J.; Zíková, M.; Oswald, J.; Komninou, P.; Hulicius, E.

Physical properties of hot wall deposited Sn1-XPbXS thin films

Nanosystems: Physics, Chemistry Mathematics

2014

Gremenok, V. F.; Ivanov, V. A.; Izadneshan, H.; Lazenka, V. V.; Bakouie, A.

Microstructure and dielectric properties of BaTiO3 ceramic doped with yttrium, magnesium, gallium and silicon for AC capacitor application

Materials Research Bulletin

2014

Wang, M. J.; Yang, H.; Zhang, Q. L.; Lin, Z. S.; Zhang, Z. S.; Yu, D.; Hu, L.

Evidence of dislocation cross-slip in MAX phase deformed at high temperature

Scientific Reports

2014

Guitton, A.; Joulain, A.; Thilly, L.; Tromas, C.

Formation of amorphous phase with crystalline globules in Fe–Cu–Nb–B immiscible alloys

Journal of Alloys and Compounds

2014

Nagase, T.; Suzuki, M.; Tanaka, T.

Ceramic-metallic (TiN-Cu) nanostructured ion-plasma vacuum-arc coatings for cutting hard-alloy tools

Russian Journal of Non-Ferrous Metals

2014

Blinkov, I. V.; Volkhonskii, A. O.; Laptev, A. I.; Sviridova, T. A.; Tabachkova, N. Yu.; Belov, D. S.; Ershova, A. V.

Designing active and stable silicon photocathodes for solar hydrogen production using molybdenum sulfide nanomaterials

Advanced Energy Materials

2014

Benck, J. D.; Lee, S. C.; Fong, K. D.; Kibsgaard, J.; Sinclair, R.; Jaramillo, T. F.

Observation of the atomic structure of ß′-SiAlON using three generations of high resolution electron microscopes

Philosophical Magazine A

2013

Thorel, A.; Ciston, J.; Bartel, T.; Song. C. Y.; Dahmen, U.

Optimized Ar+-ion milling procedure for TEM cross-section sample preparation

Ultramicroscopy

2011

Dieterle, L.;Butz, B.; Müller, E.